World Leader in Nitrogen Gas Analyzers


Home Contact Us K2001 K2002 K3000 Sample Systems Purifiers Newsletter



General description
The gas at atmospheric pressure, flows through a proprietary design ; a pure quartz cell is submitted to a high-frequency, high-intensity electromagnetic field.

The K2001 Analyzer is based on a spectroscopic emission cell, which is not a new technique in itself. Rather, it is the frequency, the intensity, the regulation as well as the coupling technique and focusing (stabilizing) electrodes used to keep the plasma stable that make this system stable and selective.

 

Under these conditions, it becomes the center of a luminous phenomenon (electroluminescence). In fact, this is an electromagnetically induced plasma. A plasma is a collection of charged particles ; In this case, the plasma consists of a stream of argon. This process being an emission technique, it is very useful for quantitative analysis. This technique is not new, but the recent advances in semiconductors as well as in optical coating and devices, make it easier to develop an instrument based on this technology, without the cost normally associated with this category of analytical instruments.

Once the gas is ionized (charged), many spectral lines are emitted.

Here, we think a few words regarding the technique used to create the plasma are necessary. There are many ways of producing light from an argon stream for analytical purposes. The electroluminescence phenomenon includes luninescence from all kinds of electrical discharges, such as sparks, arcs or tubes of different kinds, operating on direct or alternating current of low or high frequency. Recently, some experiments were conducted in the microwave range by surface-wave-induced plasma.

Excitation in these cases results mostly from electron or ion collisions ; it is the kinetic energy of electrons or ions accelerated in an electric field to which the atoms or molecules of the gas are subjected that causes emissions of light.

By any of the previous methods, characteristic emission spectra can be obtained for argon and each substance in it. They usually vary for a given substance, depending on the mode of excitation.

We developed our plasma generator and plasma cell as to minimize the heat generation inside the cell and get a clear spectral line for the substance of interest, i.e. nitrogen.

Once the intense line is identified, we must use a system to filter it out. In our case, instead of a grating, prism or tunable filter, we use an custom made optical filter with special coating that lessens background noise considerably and reduces spectral interference. This filter show an exceptional bloking range. Its main characteristic is its great stability : temperature and humidity and time will not affect its performance it is coupled with a special lens that focuses the optical beam.

The resulting light is directed to a special photodiode, where an electrical current is generated. This current is proportional to the nitrogen level in the gas stream. (Argon or helium).

By regulating the power of the plasma and having close control of plasma position, with the focusing electrodes, we can optimize the sensitivity for a particular spetral ray.



Features
  • Measuring system based on light emission of an argon plasma maintened in a quartz chamber, controlled by a microprocessor system
  • Easy to operate
  • Solid state mass flow controller
  • Low sample flow (works with as low as 25 sccm)
  • Low power (35 watts)
  • No valves, columns, or carrier gas
  • No radioactive source
  • No moving parts, all solid state
  • No sensor or detector to replace
  • Maintenance free
Applications
  • Electronic wafer fabs
  • Gas management system
  • Gas purifier efficiency monitoring
  • Specialty gas laboratories
  • High purity Argon plant


Specifications

Detector type :
Single beam. Electromagnetically induced plasma cell.
Material : Quartz, single element, vacuum tight to 10 PSI (69 kPA).
Range :
0 - 1 ppm, resolution to 10 ppb
0 - 10 ppm, resolution to .1 ppm
0 - 100 ppm, resolution to 1 ppm
Accuracy :
Better than ± 1 % of full scale
Sample flow requirements :
30 to 150 sccm
Gas connections :
Sample : 1/8" swagelok tube fitting
Vent : 1/8" swagelok tube fitting
Recommended calibration gas :
Zero : 1.0 to 2.0 ppm N2/Ar
Span : 8.0 to 9.5 ppm N2/Ar (for 0 - 10 Pppm range)
Flow accuracy :
0 to 200 sccm ± 1 % full scale
Maximum input pressure :
70 PSIG (482 kPAG) (vent at atmospheric pressure)
Recommended operating input pressure :
5 PSIG to 10 PSIG (35.5 kPAG to 69 kPAG)
Operating temperature :
10° C to 35° C
Supply :
115 VAC, 50 - 60 Hz or 220 VAC, 50 - 60 Hz
Power consumption :
Maximum 35 watts
Response time :
20 seconds for 90 % of a step change at 75 sccm (typically 10 seconds)
Drift :
± 1 % over 24 hours (typically ± .5 % over long term)
Weight :
15 kg (33lbs)
Standard features :
  • Microprocessor controlled with 4 X 40 LCD display
  • Self diagnostic system software
  • Manual or autoranging (user selectable)
Options :
  • Auto-zero, auto-span calibration, done at user preselected interval
  • Digital outputs for remote monitoring : (all dry relay contacts, SPST 1 amp 250 Vac resistive load)
    • System status (1 output)
    • Range in use (3 outputs)
    • 2 alarm outputs (user programmable set point)
  • 4 - 20 mA isolated output
    Maximum load impedance : 600 ohms at 20 mA DC
    Isolation : 750 VDC or AC peak maximum
  • Serial port : RS-232 / 422 / 485 / modem
  • Custom option : contact factory
and UL1244 compliant